Thursday, July 29, 2010

Synthesis and characterization of mono-dispersed Y3Al5O12:Er3+-coated SiO2 nanoparticles by co-precipitation process

Synthesis and characterization of mono-dispersed Y3Al5O12:Er3+-coated SiO2 nanoparticles by co-precipitation process: "

Abstract  
In this paper, a facile co-precipitation process for preparing mono-dispersed core–shell structure nanoparticles is reported.
The 110 nm SiO2 cores coated with an yttrium aluminum garnet (Y3Al5O12) layer doped with Er3+ were synthesized and the influence of the concentration ratio of [urea]/[metal ions] on the final product was investigated.
The structure and morphology of samples were characterized by the X-ray powder diffraction, Fourier transform IR spectroscopy
and transmission electron microscopy, respectively. The results indicate that a layer of well-crystallized garnet Y3Al5O12:Er3+ were successfully coated on the silica particles with the thickness of 20 nm. The near infrared and upconversion luminescent
spectra of the SiO2@Y3Al5O12:Er3+ powders further confirm that a Y3Al5O12:Er3+ coating layer has formed on the surface of silica spherical particles.

  • Content Type Journal Article
  • Category Research Paper
  • DOI 10.1007/s11051-010-0036-x
  • Authors
    • Cheng-Ning Xie, South China University of Technology Key Lab of Specially Functional Materials of Ministry of Education and Institute of Optical Communication Materials Guangzhou 510641 People’s Republic of China
    • Zhong-Min Yang, South China University of Technology Key Lab of Specially Functional Materials of Ministry of Education and Institute of Optical Communication Materials Guangzhou 510641 People’s Republic of China
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