Tuesday, June 08, 2010

Luminescence property of Ca3(VO4)2:Eu3+ dependence on molar ratio of Ca/V and solution combustion synthesis temperature

Luminescence property of Ca3(VO4)2:Eu3+ dependence on molar ratio of Ca/V and solution combustion synthesis temperature: "

Abstract  
Red emitting phosphor Ca3(VO4)2:Eu3+ was prepared by citric acid-assisted solution combustion method and characterized by X-ray diffraction (XRD), transmission
electron microscopy (TEM), and fluorescence spectrophotometer. The influences of Ca to V molar ratio and synthesis temperature
on phase composition, morphology, grain size, photofluorescence properties, and ultraviolet–visible diffuse reflectance spectra
(UV–Vis DRS) of as-synthesized samples were investigated. The results indicate that Ca to V molar ratio play a key role for
the changing of phase composition, excitation spectrum, and luminescence intensity. The sample prepared at 900 °C, keeping
Ca/V = 3:2.2, has the highest photoluminescence intensity. The possible causes of the effects on photoluminescence mechanism
were also discussed in this work.

  • Content Type Journal Article
  • DOI 10.1007/s10853-010-4598-x
  • Authors
    • Kehui Qiu, Chengdu University of Technology Institute of Materials Science and Technology Chengdu 610059 Sichuan People’s Republic of China
    • Junfu Li, Chengdu University of Technology Institute of Materials Science and Technology Chengdu 610059 Sichuan People’s Republic of China
    • Junfeng Li, Chengdu University of Technology Institute of Materials Science and Technology Chengdu 610059 Sichuan People’s Republic of China
    • Xueguang Lu, Chengdu University of Technology Institute of Materials Science and Technology Chengdu 610059 Sichuan People’s Republic of China
    • Yingchun Gong, Chengdu University of Technology Institute of Materials Science and Technology Chengdu 610059 Sichuan People’s Republic of China
    • Junhan Li, Chengdu University of Technology Institute of Materials Science and Technology Chengdu 610059 Sichuan People’s Republic of China
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